Versatile synthesis and enlargement of functionalized distorted heptagon-containing nanographenes† †Electronic supplementary information (ESI) available: General details, synthesis and spectroscopy data of new compounds and copies of 1H and 13C-NMR spectra of new compounds. Experimental details on optical and electrochemical measurements. Crystal data and structure refinement of compounds 2, 6a, 6d and 6h. Further details on theoretical calculations and Cartesian coordinates of computed structures. VT-1H-NMR, 2D-NMR and HRMS spectra of compounds 1 and 2. CCDC 1485682–1485685. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6sc02895k Click here for additional data file. Click here for additional data file.
نویسندگان
چکیده
a. Departamento Química Orgánica, Universidad de Granada (UGR). C. U. Fuentenueva,18071 Granada, Spain. email: [email protected], [email protected] b. Departamento de Fisicoquímica, Facultad de Farmacia, UGR. Cartuja Campus, 18071 Granada, Spain. c. Departamento de Química Orgánica I, Universidad del País Vasco, E-20018, San Sebastián (Spain) d. Departamento de Química, Universidad Autónoma de Madrid. c/Francisco Tomás y Valiente no 7, Cantoblanco, 28049 Madrid, Spain. e. Laboratorio de Estudios Cristalográficos, Instituto Andaluz de Ciencias de la Tierra (CSIC-UGR), 18100 Armilla, Granada, Spain. f. Departamento de Electrónica y Tecnología de Computadores. Facultad de Ciencias, CITIC, UGR, E18071 Granada. (Spain) g. Fundación IMDEA Nanociencia. Ciudad Universitaria de Cantoblanco, E-28049 Madrid. (Spain) h. Institute of Chemical Research of Catalonia (ICIQ). Catalan Institution for Research and Advanced Studies (ICREA)
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Optical and electronic properties of air-stable organoboron compounds with strongly electron-accepting bis(fluoromesityl)boryl groups† †Electronic supplementary information (ESI) available: Experimental details. Additional views of the molecular structures from X-ray diffraction. Cyclic voltammograms of 2 and 3. Plots of calculated lowest energy transitions versus UV-visible absorption spectra. Variable-temperature emission and excitation spectra. Copies of all NMR spectra. Cartesian coordinates of all optimised geometries. CCDC 1010408–1010412. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c4sc02410a Click here for additional data file. Click here for additional data file.
Institut für Anorganische Chemie, Julius Hubland, 97074 Würzburg, Germany. E-ma School of Medicine, Pharmacy and Health, Stockton-on-Tees, TS17 6BH, UK Department of Chemistry, University of Tor M5S 3H6, Canada Institut für Organische Chemie, JuliusHubland, 97074 Würzburg, Germany † Electronic supplementary information Additional views of the molecular stru voltammograms of 2 and 3. Plots of ca...
متن کاملEnhanced intersystem crossing in core-twisted aromatics† †Electronic supplementary information (ESI) available: Includes details of the synthesis, structural information for all of the compounds (NMR, elemental analysis and mass spectra) and experimental details for the photophysical studies. CCDC 1402604 and 1402605. For ESI and crystallographic data in CIF or other electronic formats see DOI: 10.1039/c6sc05126j Click here for additional data file. Click here for additional data file.
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عنوان ژورنال:
دوره 8 شماره
صفحات -
تاریخ انتشار 2017